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Sb 2 Se 3, SnSe, SnSe 2, SnSb 2 Se 4, and Sn 2 Sb 6 Se 11 were prepared from powdered elements in a planetary ball mill. The progress of the reactions was investigated in situ by difference thermoanalysis and ex situ by X-ray analyses. SnSb 2 Se 4, and Sn 2 Sb 6 Se 11 are probably both positioned in the homogeneity region of the only ternary compound of the system Sn–Sb–Se.

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